Dairy Based Precursor Formulation for Whippable Topping or Dessert Filling

ABSTRACT

A precursor formulation for a whippable dessert topping or filling comprises milk solids and dairy fats, and has a water phase which comprises bovine-derived water such as skim milk, whole milk, or buttermilk, or treated water having a pH and mineral content similar to bovine-derived water, in which skim milk solids have been dissolved; and a dairy fat/solids phase which has SFI characteristics similar to those of natural butterfat. The formulation comprises water phase of 50% to 80% by weight; dairy fat, 12% to 35%, sugar, 10% to 12%; salt, 0.1% to 0.2%; lecithin and flavor, each 0.3% to 0.5%; and gums, 0.5% to 1.0%. A method of preparation of the precursor formulation includes mixing, heating, pasteurization, high pressure homogenization, cooling, high pressure re-homogenization, and packaging.

FIELD OF THE INVENTION

This invention relates to dessert toppings and fillings, and particularly to dessert toppings and fillings that are whippable or in some circumstances that have been whipped. Particularly, the present invention relates to a precursor formulation for the whippable dessert toppings and fillings which can later be whipped or aerated for their particular use as a dessert topping or for fillings in pies and cakes. The precursor formulation for whippable dessert toppings and fillings in keeping with the present invention is an all dairy product, employing only bovine-derived water, butterfat, and/or cream, in its formulation. Moreover, the precursor formulation for whippable dessert toppings and fillings in keeping with the present invention allows for simple product labeling whereby the consumer can be assured of a healthier, all dairy product, than heretofore available. A tub-packed whipped topping is one of the resultant consumer products that may derive from the present invention.

BACKGROUND OF THE INVENTION

Whipping cream has been used with various kinds of desserts and cooling as a topping for fruits and the like and as a filling for various kinds of cakes and pies. The use of whipping cream as a complement to the enjoyment of any dessert has probably been known for centuries. Indeed, up until the Second World War, whipping cream was very popular. However, during the war access to dairy products became limited, and all dairy products were in short supply. During the war, replacement products were brought to the market, and they typically employed various kinds of vegetable oils together with suitable and appropriate emulsifiers. However, while acceptable and used, such replacement dessert toppings were not wholeheartedly received, since they had relatively poor taste and their mouth feel was unappetizing.

After the war, rich desserts once again became fashion, and the use of whipping cream increased. By the 1970s, however, health concerns became more prominent, and many people began to worry about their intake of rich and fatty foods, their increase in cholesterol levels, and the impact of those matters on their general well-being. Moreover, the cost of dairy products was again increasing compared with other staple foods. Still further, the retail or consumer market was demanding the supply of whipped toppings packaged in tubs, giving rise to the supply of vegetable oil based products that were high in chemically altered fat systems with significant quantities of hydrogenated fats and trans-fatty acids.

Of course, it has been determined that hydrogenated fats and trans-fatty acids are more detrimental to human health then naturally occurring saturated fats such as those found in butterfat. Nonetheless, there are still several mitigating factors that suggest that there is still very widespread acceptance and desire in the market to consume dessert toppings and fillings that are prepared with cream or butterfat. Still further, increased demand for such products, and the economics of bringing such products to the market, leads to the conclusion that a healthier and cost-effective solution must be found so as to replace unacceptable reliance on hydrogenated fats and trans-fatty acids.

On the other hand, it must also be recognized that manufacturers of dairy products, and consumers of manufactured dairy products, are subject to the vagaries of supply and price which are concomitant with changes of season. This may lead to the rather unexpected circumstances that at some times in the year the price of butter may be cheaper than the price of dairy cream. Moreover, the dairy industry as such that skim milk is always available. By referring to “butter”, it will be understood that the reference is generally to unsalted butter.

In any event, the present inventor has unexpectedly determined that it is possible to provide a precursor formulation for whippable edible products which may be employed as dessert toppings and fillings, and which has a significant dairy constituent. To that end, as will be discussed in greater detail hereafter, the present invention provides a formulation for whippable dessert toppings and fillings that has a significant water phase and a dairy fat/solids phase which will emulate in all respects natural whipping cream, but which will have significant shelf life and can be brought to the market economically.

One novel aspect of the present invention is that, in certain principal embodiments thereof, the inventor herein employs bovine-derived water, which means that the water phase of the precursor formulation is derived from dairy products. That means that the water content of liquid milk as it comes from dairy cattle and after it has been treated either to make buttermilk or skim milk has come to the attention of the inventor as being a suitable source of milk solids. It will be understood, of course, that skim milk or buttermilk will contain 3% up to 12% of non-fat skim milk solids or buttermilk solids dissolved therein, thus providing the source of milk solids as noted immediately above.

However, it must at this time be stressed that by “buttermilk”, what is meant is that product which remains in a butter churn after butter has been removed therefrom. Real buttermilk production is tied, of course, to the production of butter. Thus, as noted above, there may be some seasonal variation in the costs and availability of buttermilk. However, essentially the same milk solids may also be found in skim milk from which all butterfat has been removed. Therefore, the use of bovine-derived water as the water phase of the precursor formulation of the present invention is an important feature in certain principal embodiments thereof.

Moreover, it will also be stressed that store-bought buttermilk is not the same as real buttermilk. Rather, store-bought buttermilk is a cultured skim milk which has been acidified. Thus, the use of store-bought buttermilk is not at all contemplated by the present invention, and is contrary to the purposes and goals of the present invention.

However, the present invention also contemplates the emulation of bovine-derived water by the provision of specially treated water which has been treated so as to have a pH and a mineral content similar to the water constituent of bovine-derived water such as that discussed above with respect to skim milk and buttermilk. But it must be noted that for use as the water phase in the formulation of the present invention, it is necessary as well to provide the necessary skim milk solids or buttermilk solids so as to effectively emulate skim milk or buttermilk. As a practical matter, the water must first be treated to adjust its pH and its mineral content to emulate that of bovine-derived water, after which skim milk powder or buttermilk powder is added. This is because, as a general rule, skim milk powders or buttermilk powders do not easily dissolve in water; or at least, the lactose and protein milk solids found in dried skim milk powder or buttermilk powder will not easily dissolve in water that has not at least been treated as to its pH to improve its affinity for the skim milk or buttermilk solids.

Moreover, as will be noted hereafter, the present invention also contemplates that in some circumstances, the liquid water phase of the precursor formulation, and a certain portion of the dairy fat/solids phase of the formulation may be derived from whole milk, provided that the water phase and dairy fat constituents within the formulation satisfy the permissible ranges therefor.

The present invention further contemplates that the precursor formulation for a whippable dessert topping or filling may be fortified by the addition of extra calcium that has been derived from milk. This is typically achieved in the dairy industry for drinking milk (usually, partially skimmed milk) by the addition of modified milk solids, but has been hitherto unknown for creams, and particularly whipping creams and the like.

More especially, the present invention seeks to provide the consumer with an enjoyable dessert product having flavor and mouth feel, whipping characteristics, and stability, similar to those of real whipped cream having approximately 35% butterfat; and at the same time to provide a healthy product that has a standardized dairy fat content, but is not subject to the seasonal vagaries of the dairy market.

DESCRIPTION OF THE PRIOR ART

The inventor herein is the author of a number of patents which relate in one way or another to milk products. They include U.S. Pat. No. 5,672,373 relating to the production of dry milk powder which has a fat content equivalent to that of dry whole milk; and U.S. Pat. No. 6,620,451 which relates to the preparation of a recombined cream formulation.

Another patent relating to a method for making a whipped cream filler having a milk fat constituent is Herrmann U.S. Pat. No. 5,494,694.

A series of patents which particularly relate to various technologies surrounding a commercial whipped topping composition, which may or may not comprise milk fat and which rely heavily on the use of hydrogenation, emulsifiers, cross-linked starches, and the like, includes U.S. Pat. Nos. 4,251,561; 4,451,492; 4,505,943; 5,077,076; 5,384,146; and 5,384,145.

SUMMARY OF THE INVENTION

The present invention provides a precursor formulation for a whippable dessert topping or filling which will comprise milk solids and dairy fats, and which has a water phase and a dairy fat/solids phase.

The water phase of the precursor formulation of the present invention may comprise bovine-derived water chosen from the group which consists of skim milk, whole milk, buttermilk derived from a butter churn, and mixtures and combinations thereof, and has 3% to 12% by weight of dissolved skim milk or buttermilk solids therein.

Alternatively, the water phase of the precursor formulation of the present invention may comprise treated water which has a pH and mineral content similar to the water constituent of bovine-derived water, and to which skim milk or buttermilk solids have been added to the same extent as occurs in ordinary skim milk or buttermilk. Accordingly, this water phase also has 3% to 12% by weight of dissolved skim milk or buttermilk solids therein.

The dairy fat constituent of the dairy fat/solids phase has SFI characteristics similar to those of natural butterfat. The dairy fat constituent is chosen from the group consisting of butterfat, dairy cream, and mixtures and combinations thereof;

The formulation is as follows:

water phase 50% to 80% by weight dairy fat 12% to 35% by weight sugar 10% to 12% by weight salt 0.1% to 0.2% by weight lecithin 0.3% to 0.5% by weight flavor 0.3% to 0.5% by weight gums 0.5% to 1.0% by weight emulsifier 0.5% to 3.0% by weight

Moreover, the SFI characteristics of the dairy fat constituent of the dairy fat/solids phase are as follows:

10° C. 40% to 43% 20° C. 21% to 22% 30° C. 5.5% to 7.5% 40° C. 0%

Still further, the formulation of the present invention may in some circumstances comprise up to an additional 10% by weight of skim milk solids.

If so, then the additional skim milk solids are added to the formulation by the addition of condensed skim milk.

Moreover, the formulation of the present invention may further comprise additional calcium content, where the calcium has been derived from milk and has been added to the formulation by the addition of modified milk solids thereto.

The present invention also provides a method for the preparation of the precursor formulation hereof, wherein the method comprises the steps of:

(a) Mixing together the ingredients of the formulation and heating the same to a temperature of at least 78° C. so as to melt and dissolve the fat and solids ingredients. (b) Blending the melted ingredients. (c) Pasteurizing the blended ingredients at a temperature of at least 80° C. (d) Homogenizing the pasteurized and blended ingredients at a temperature of at least 75° C. and at a pressure of 1000 psi to 7000 psi. (e) Cooling the homogenized mixture to a temperature of 25° C. to 45° C. (f) Re-homogenizing the cooled mixture at a temperature of 25° C. to 45° C. and at a pressure of 1000 psi to 7000 psi. (g) Placing the re-homogenized mixture in containers and maintaining the same at a temperature of 10° C. to 45° C.

The containers which are chosen may be such as tanks, drums, aerosol containers, and combinations thereof.

The method of the present invention may further comprise the following steps:

(h) Electively, whipping the cooled, re-homogenized mixture in whipping machine, or infusing the cooled re-homogenized mixture with a cryogenic gas, so as to entrain air therein and thereby so as to prepare a formulation having a predetermined specific gravity. (i) Packaging the whipped formulation in predetermined quantities. (j) Storing the packaged formulation at temperatures of −15° C. to 0° C.

It should be noted that when the product has been whipped so as to entrain air therein, then prior to step (j) the temperature of the package product is quickly reduced to below 0° C.

Finally, it is emphasized once again that the liquid water phase as it is employed in the methods of the present invention and in the preparation of the formulation in keeping with present invention may be bovine-derived water chosen from the group consisting of skim milk, whole milk, buttermilk derived from a butter churn, and mixtures and combinations thereof; or it may be treated water having a pH and mineral content similar to the water constituent of bovine-derived water, and to which skim milk solids have been added to the same extent as occurs in ordinary skim milk, whole milk, or buttermilk. In all events, the water phase will have 3% to 12% by weight of dissolved skim milk or buttermilk solids therein.

DETAILED DESCRIPTION OF THE INVENTION

The novel features which are believed to be characteristic of the present invention, as to its structure, organization, use and method of operation, together with further objectives and advantages thereof, will be better understood from the following discussion.

The formulation of the precursor for a whippable dessert topping or filling in keeping with present invention has been provided above. However, to reiterate what that formulation is, for purposes of the present discussion, it is as follows:

water phase 50% to 80% by weight dairy fat 12% to 35% by weight sugar 10% to 12% by weight salt 0.1% to 0.2% by weight lecithin 0.3% to 0.5% by weight flavor 0.3% to 0.5% by weight gums 0.5% to 1.0% by weight emulsifier 0.5% to 3.0% by weight

Some discussion of each of the constituent components of the formulation is now given. First, it has been noted that the water phase of the formulation in keeping with present invention may comprise bovine-derived water which is typically skim milk, whole milk, or buttermilk which has been derived from a butter chum. Mixtures and combinations of those may also be employed. Alternatively, it has been noted that the water phase may be substituted by specially treated water which has been so treated so as to have a pH and mineral content similar to the water constituent of bovine-derived water, and to which skim milk or buttermilk solids have been added to the same extent as they will occur in ordinary skim milk. It is this water phase to which the other ingredients which comprise the dairy fat/solids phase are mixed and blended. In all events, the water phase has 3% to 12% by weight of dissolved skim milk or buttermilk solids therein.

The dairy fat constituent of the dairy fat/solids phase is chosen from the group consisting of butterfat, dairy cream, and mixtures thereof, and will provide SFI characteristics similar to those of natural butterfat, namely:

10° C. 40% to 43% 20° C. 21% to 22% 30° C. 5.5% to 7.5% 40° C. 0%

Thus, the dairy fat constituent will have significant solids content at 10° C. and zero solids content at 40° C. Accordingly, the remaining constituents which comprise the dairy fat/solids phase of the formulation in keeping with present invention may be melted and dissolved into the water phase at elevated temperatures. Then, upon homogenization and cooling, a whippable product which, upon whipping, will have a mouth feel similar to that of whipped cream, is provided.

It is a provision of the present invention, therefore, no matter what the source of dairy fat may be the butterfat constituent thereof will be standardized so as to provide the SFI characteristics noted above. In other words, if the water phase comprises whole milk—which typically has about 3.5% fat as opposed to dairy cream which may have up to 35% fat—a suitable adjustment which is well known to those skilled in dairy fat arts would be made so as to arrive at a formulation which comprises 12% up to 35% by weight of dairy fat. Also, as noted, the dairy fat constituent may be derived from butterfat—typically, unsalted butter—or dairy cream, and combinations thereof, so that of the dairy cream is derived from whole milk it will enter into the calculation of the formulation so as to result in a standardized fat content. As to be noted hereafter, that fat content may be chosen so as to provide so-called “low fat” formulations, or formulations that emulate real whipping cream having 35% butterfat content.

The addition of the remaining solids provides for the necessary sweetness, flavor, stability, and shelf life of the precursor formulation and/or the whipped dessert topping or filling which is produced therefrom. The purpose of the sugar and salt, and flavor, is self-evident; the purpose of the lecithin, gums, and emulsifier is to provide for shelf life and stability. These additional constituents, however, do not affect the storing or eating characteristics of the product. Moreover, the specific choice of flavor, gums, and emulsifier, is beyond the scope of the present invention but it will be evident to those skilled in the art that any suitable flavor such as vanilla extract or the like, and any suitable gums such as guar, carrageenan, xanthan, and mixtures and combinations thereof, may be employed. The emulsifier must be such that it is compatible with the non-fat milk solids, dairy fat, and other constituents that are employed in formulations according to the present invention.

It has been noted that the dairy fat constituent may be in a range of from 12% up to 35%. Typical “low fat” formulations of whipped toppings, and whipping cream sold in aerosol containers, comprise from 17% to 22% fat composition, but may be somewhat lower in some circumstances. In that case, it may be appropriate to add additional skim milk solids; and particularly, it may be appropriate to add condensed skim milk in order to provide for the addition of the further solids which might be required. If so, then condensed skim milk will form part of the water phase of the formulation of the present invention. Moreover, modified milk solids may be added, if required, to provide a higher calcium content than would otherwise occur; it being noted, however, that the additional calcium content is natural, and has been milk-derived.

Real whipping cream typically comprises approximately 35% butterfat, and the intention of the present invention is to emulate that fat content, particularly in circumstances where richness of the dessert topping or filling is desired.

Still further, the fat composition constituent of the formulations in keeping with present invention may be structured having a full comprehension of the polymorphic behavior of the fats in the formulation in order to create emulsion stability and to control the latent heat release of the product when it is cooled; and particularly, when it is frozen. Otherwise the air holding capacity and stability of the whipped product may be compromised.

It will be appreciated by those skilled in the art that when non-fat milk solids are added to a dairy fat system, in keeping with present invention, each incremental addition of solids will affect the firmness of the fat system in such a manner that the increasing firmness is essentially logarithmic in nature.

In carrying out the method of the present invention, it is noted that the first step is to mix all the ingredients of the formulation together and to heat the same to at least 78° C., so as to melt and dissolve the fat and solids ingredients. At same time, all the constituents are blended together. Then, the blended ingredients will be pasteurized at a temperature of at least 80° C. While the blended ingredients are still hot, at least above 75° C., they are then homogenized at a homogenization pressure of at least 1000 psi up to 7000 psi. All of those steps and the machinery that is used for them are well known to those skilled in the dairy arts, and particularly to those having experience with the production of whipped dairy products.

After the first homogenization step the product is then cooled to a temperature of 25° C. to 45° C. Thereafter, it is once again homogenized while at that lower temperature; and once again it is homogenized at pressures of 1000 psi to 7000 psi.

After the second homogenization step, the homogenized precursor formulation may then be packaged or placed in suitable containers and kept at temperatures not below 10° C. and not above 45° C. This homogenized precursor formulation finds a very ready market with commercial bakeries, hotels, and restaurants. There, the product will be used in the preparation of various desserts and baked goods which require a whipped topping or a whipped filling which will emulate the appearance, flavor, and mouth feel, of real whipped cream.

Other consumers of the homogenized precursor formulation may be producers of a whipped dessert topping of the sort sold in the retail market to household consumers.

Thus, appropriate containerization for the homogenized precursor formulation when in its unwhipped condition may be such as tanks or drums in which large quantities may be delivered. On the other hand, the homogenized precursor formulation may also be placed into aerosol cans to be dispensed as a whipped topping, in particular; in which case it may find customers in both the commercial and retail markets.

At this time comment must be emphasized that because the formulation does not employ any fat system apart from fats that are derived from milk, any product in keeping with present invention that is applied to any bakery, commercial, or retail customer, may be labeled as being “all dairy” or other such terminology which will teach and imply that the product has no vegetable oils of any sort in its formulation.

When the product is whipped by being aerated in such as a Votator™ or other whipping machine, typically air is entrained into the product. If so, then it may be desirable for the whipped product to be packaged in individual small packages such as plastic tubs which are then sealed and treated in such a manner that the temperature of the packaged product is quickly reduced to below 0° C. This assures that surface area of the whipped product, and thus its overrun with respect to the original volume of the homogenized precursor formulation, remains stable; and the increased surface area of the whipped product decreases the freezing time.

The homogenized precursor formulation of the present invention may also be treated by infusing the formulation with a cryogenic gas—typically, carbon dioxide—in which case the presence of a cryogenic gas assists in freezing the product. Moreover, the use of a cryogenic gas will assure control of the overrun and air intake into the whipped product. Thus, freezing time will be less due to the presence of the cryogenic gas, but it may be dependent on the size of the air/gas bubbles in the product. As before, this product may be packaged in individual small packages such as plastic tubs which are sealed and stored at temperatures below 0° C.

EXAMPLE 1

A precursor formulation in keeping with present invention had the following specific formula:

buttermilk/skim milk water phase  60% by weight dairy fat  25% by weight sugar 13.7% by weight  salt 0.1% by weight lecithin 0.3% by weight flavor 0.3% by weight gums 0.4% by weight emulsifier 0.2% by weight

The formulation was manufactured in keeping with the steps of the present invention, as described above. The homogenization pressure at each of the hot and cool homogenization steps was 6000 psi.

The formulation had very good whippability and mouth sense, and was no different in any subjective test than real whipping cream. The whipped product exhibited excellent air entertainment and stability, and could be substituted for whipped cream in eating tests.

There has been described typical formulations for a whippable dessert topping or filling which comprises milk solids and dairy fats, and which emulates real whipping cream as to color, taste, and mouth feel. The precursor formulation of the present invention will provide a whipped product which emulates real whipped cream. It will be understood and appreciated that other modifications and variations to the formulations in keeping with present invention, and its method of production, will be evident to those skilled in the art and may be employed without, however, departing from the spirit and scope of the present claims.

Throughout this specification and the claims which follow, unless the context requires otherwise, the word “comprise”, and variations such as “comprises” or comprising, will be understood to imply the inclusion of a stated integer or step or group of stated integers or steps, but not to the exclusion of any other integer or step or group of integers or steps. It will also be understood that phrases such as “similar to” and “to the same extent” imply properties and ranges which are not dissimilar to those to which they have been compared, but which are not necessarily exactly the same. 

1. A precursor formulation for a whippable dessert topping or filling comprising milk solids and dairy fat, and having a water phase and a dairy fat/solids phase; wherein said precursor formulation is intended for storage in containers in an unwhipped condition at a temperature in the range of 100° C. to 45° C., and may be transported in said containers at said storage temperature: wherein said water phase comprises bovine-derived water chosen from the group consisting of skim milk, whole milk, buttermilk derived from a butter chum, and mixtures thereof, and said water phase has 3% to 12% by weight of dissolved milk solids or dissolved buttermilk solids therein; wherein the dairy fat constituent of said dairy fat/solids phase has SFI characteristics substantially the same as those of natural butterfat, and is chosen from the group consisting of butterfat, dairy cream, and mixtures thereof; wherein said formulation comprises the following constituents: water phase 50% to 80% by weight dairy fat 12% to 35% by weight sugar 10% to 12% by weight salt 0.1% to 0.2% by weight lecithin 0.3% to 0.5% by weight flavor 0.3% to 0.5% by weight gums 0.5% to 1.0% by weight emulsifier 0.5% to 3.0% by weight

and wherein the SFI characteristics of the dairy fat constituent of said dairy fat/solids phase are: 10° C. 40% to 43% 20° C. 21% to 22% 30° C. 5.5% to 7.5% 40° C. 0%.


2. A precursor formulation for a whippable dessert topping or filling comprising milk solids and dairy fats, and having a water phase and a dairy fat/solids phase; wherein said precursor formulation is intended for storage in containers in an unwhipped condition at a temperature in the range of 10° C. to 45° C., and may be transported in said containers at said storage temperature: wherein said water phase comprises water having a pH and mineral content substantially the same as the water constituent of bovine-derived water, and said water phase has milk solids or buttermilk solids which have been added thereto to the extent of 3% to 12% by weight of dissolved milk solids or dissolved buttermilk solids therein; wherein the dairy fat constituent of said dairy fat/solids phase has SFI characteristics substantially the same as those of natural butterfat, and is chosen from the group consisting of butterfat, dairy cream, and mixtures thereof; wherein said formulation comprises the following constituents: water phase 50% to 80% by weight dairy fat 12% to 35% by weight sugar 10% to 12% by weight salt 0.1% to 0.2% by weight lecithin 0.3% to 0.5% by weight flavor 0.3% to 0.5% by weight gums 0.5% to 1.0% by weight emulsifier 0.5% to 3.0% by weight

wherein the SFI characteristics of the dairy fat constituent of said dairy fat/solids phase are: 10° C. 40% to 43% 20° C. 21% to 22% 30° C. 5.5% to 7.5% 40° C. 0%.


3. (canceled)
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 9. A method of preparation of a precursor formulation for a whippable dessert topping or filling comprising milk solids and dairy fats, and having a liquid water phase and a dairy fat/solids phase; wherein said water phase comprises bovine-derived water chosen from the group consisting of skim milk, whole milk, buttermilk derived from a butter chum, and mixtures and combinations thereof, and has 3% to 12% by weight of dissolved milk or buttermilk solids therein; wherein the dairy fat constituent of said dairy fat/solids phase has SFI characteristics similar to those of natural butterfat, and is chosen from the group consisting of butterfat, dairy cream, and mixtures and combinations thereof; and wherein said formulation comprises: water phase 50% to 76.8% by weight dairy fat 12% to 35% by weight sugar 10% to 12% by weight salt 0.1% to 0.2% by weight lecithin 0.3% to 0.5% by weight flavor 0.3% to 0.5% by weight gums 0.5% to 1.0% by weight emulsifier 0.5% to 3.0% by weight

said method comprising the steps of: (a) mixing together the ingredients of said formulation and heating the same to a temperature of at least 780° C. so as to melt and dissolve the fat and solids ingredients; (b) blending said melted ingredients; (c) pasteurizing said blended ingredients at a temperature of at least 80° C.; (d) homogenizing said pasteurized and blended ingredients at a temperature of at least 75° C. and at a pressure of 1000 psi to 7000 psi; (e) cooling said homogenized mixture to a temperature of 25° C. to 45° C.; (f) re-homogenizing said cooled mixture at a temperature of 25° C. to 45° C. and at a pressure of 1000 psi to 7000 psi; (g) placing said re-homogenized mixture in containers and maintaining the same at a temperature of 100° C. to 45° C.
 10. The method of claim 9, wherein said containers are chosen from the group consisting of tanks, drums, aerosol containers, and combinations thereof.
 11. The method of claim 9, further comprising the steps of: (h) electively whipping the cooled, re-homogenized mixture in a whipping machine, or infusing the cooled re-homogenized mixture with a cryogenic gas, so as to entrain air therein and thereby so as to prepare a formulation having a predetermined specific gravity; (i) packaging the whipped formulation in predetermined quantities; and (j) storing the packaged formulation at temperatures of −15° C. to 0° C.
 12. The method of claim 11, wherein prior to step (j), the temperature of the packaged product is quickly reduced to below 0° C.
 13. The formulation of claim 1, wherein said stored precursor formulation may be whipped to have a predetermined specific gravity, packaged in predetermined quantities, and then stored at a storage temperature in the range of −15° C. to 0° C.
 14. The formulation of claim 2, wherein said stored precursor formulation may be whipped to have a predetermined specific gravity, packaged in predetermined quantities, and then stored at a storage temperature in the range of −15° C. to 0° C. 